Voltammetric determination of α-lipoic acid using poly(Vanillin) modified platinum electrode | Kütüphane.osmanlica.com

Voltammetric determination of α-lipoic acid using poly(Vanillin) modified platinum electrode

İsim Voltammetric determination of α-lipoic acid using poly(Vanillin) modified platinum electrode
Yazar Duran, S. T., Hassine, Chedia Ben Ali, Burç, M., Güngör, Ö.
Basım Tarihi: 2020-06
Basım Yeri - University of Tehran
Konu Square wave voltammetry, Alpha-lipoic acid, Vanillin, Platinum electrode
Tür Süreli Yayın
Dil İngilizce
Dijital Evet
Yazma Hayır
Kütüphane: Özyeğin Üniversitesi
Demirbaş Numarası 2008-4226
Kayıt Numarası 4414e421-8bea-421a-bdb8-845f8a1d324d
Tarih 2020-06
Örnek Metin In the present study electrochemical detection of alpha-lipoic acid (alpha-LA) was carried out with a poly(Vanillin) modified platinum electrode p(VA)/PtE in Brinton Robinson buffer (BR) solution. The platinum electrode surface's was modified with cyclic voltammetry method. The prepared Pt electrode was characterized by cyclic voltammetry in ferrocyanide and scanning electron microscopy (SEM) images. The number of cycles and scan rate effects were studied using square wave voltammetry (SWV) in BR buffer containing 1 mM alpha-LA. The electrochemical oxidation of alpha-lipoic acid on the modified Pt electrode is influenced by the pH and it is an irreversible reaction in which one electron and one proton are transferred. Electrolyte type and pH effect were studied. The anodic peak current shows a linear increase with alpha-LA concentrations ranging from 0.03 mM to 2.00 mM at pH 5, the detection limit being of 0.025 mM. The alpha-lipoic acid quantification in synthetic urine samples was made by SWV with the modified Pt electrode.
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Voltammetric determination of α-lipoic acid using poly(Vanillin) modified platinum electrode

Yazar Duran, S. T., Hassine, Chedia Ben Ali, Burç, M., Güngör, Ö.
Basım Tarihi 2020-06
Basım Yeri - University of Tehran
Konu Square wave voltammetry, Alpha-lipoic acid, Vanillin, Platinum electrode
Tür Süreli Yayın
Dil İngilizce
Dijital Evet
Yazma Hayır
Kütüphane Özyeğin Üniversitesi
Demirbaş Numarası 2008-4226
Kayıt Numarası 4414e421-8bea-421a-bdb8-845f8a1d324d
Tarih 2020-06
Örnek Metin In the present study electrochemical detection of alpha-lipoic acid (alpha-LA) was carried out with a poly(Vanillin) modified platinum electrode p(VA)/PtE in Brinton Robinson buffer (BR) solution. The platinum electrode surface's was modified with cyclic voltammetry method. The prepared Pt electrode was characterized by cyclic voltammetry in ferrocyanide and scanning electron microscopy (SEM) images. The number of cycles and scan rate effects were studied using square wave voltammetry (SWV) in BR buffer containing 1 mM alpha-LA. The electrochemical oxidation of alpha-lipoic acid on the modified Pt electrode is influenced by the pH and it is an irreversible reaction in which one electron and one proton are transferred. Electrolyte type and pH effect were studied. The anodic peak current shows a linear increase with alpha-LA concentrations ranging from 0.03 mM to 2.00 mM at pH 5, the detection limit being of 0.025 mM. The alpha-lipoic acid quantification in synthetic urine samples was made by SWV with the modified Pt electrode.
Cilt 12
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